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标题: 高效液相色谱法测定肩周胶囊中5-O-甲基维斯阿米醇苷含量
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作者: 凌希
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关键字词: 5—O-甲基维斯阿米醇苷 肩周胶囊 高效液相色谱法 含量测定
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摘要: 目的测定肩周胶囊中5-O-甲基维斯阿米醇苷的含量。方法采用高效液相色谱法,色谱柱为C18柱(200mm×4.6mm,5μm),流动相为乙腈-0.1%磷酸溶液,检测波长250nm。结果5—O-甲基维斯阿米醇苷进样量在0.05—0.50μg范围内与峰面积线性关系良好,加样回收率为98.76%,RSD为0.49%。结论高效液相色谱法快速、准确,可用于肩周胶囊的质量控制:[著者文摘]
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