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标题: 高效液相色谱法测定蒙药暖宫七味散中丁香酚含量
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作者: 吴军侠[1] 赵红侠[2]
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关键字词: 高效液相色谱法 暖宫七味散 丁香酚 含量测定
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摘要: 目的建立测定暖宫七味散中丁香酚含量的高效液相色谱法。方法色谱柱为Shim—pack C18柱(250mm×4.6mm,5μm),流动相为甲醇-水(58:42),流速为1.0mL/min,检测波长为280nm。结果丁香酚进样量在0.4064~8.128μg范围内与峰面积呈良好的线性关系(r=0.9993);平均回收率为98.18%,RSD=1.27%(H=6)。结论该方法简便、快速、准确,可用于暖宫七味散的质量控制。[著者文摘]
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